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Mass Transfer Lab

Simple Batch Distillation

AEC-MSTL-008

A simple batch distillation unit for studying the Rayleigh equation and separation of binary liquid mixtures.

#BatchDistillation#RayleighEquation#BinaryMixture#DistillationBasics
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Overview

The Simple Batch Distillation apparatus heats a binary liquid mixture in a flask, collects distillate fractions at different times, and measures their compositions to study the variation of distillate composition as the still-pot composition changes. This is the simplest form of distillation without any reflux or rectification. Students validate the Rayleigh equation relating initial and final still compositions to the integral of the equilibrium relationship. The experiment provides fundamental understanding of batch distillation operations used in pharmaceutical, specialty chemical, and essential oil industries where flexibility and small batch sizes are required.

Specifications

Flask capacity2 to 5 litres
Heaterelectric mantle, 0 to 500W
CondenserLiebig type, water cooled
Distillate receivergraduated glass cylinders
Temperaturethermocouple at still head
Samplingtimed fractions of distillate
Composition analysisrefractometer / hydrometer
Power supply220V AC, 50 Hz